labcol vario 4000 (Gilson Inc)

Gilson Inc is a verified supplier

Gilson Inc manufactures this product

About

News

Press Release

Team

Advisors

Partners

Contact

Bioz Stars

Bioz vStars

Buy from Supplier

Structured Review

Gilson Inc labcol vario 4000
Labcol Vario 4000, supplied by Gilson Inc, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/labcol+vario+4000/labcol+vario+4000/us11492358-4749-8-8
Average 90 stars, based on 1 article reviews

labcol vario 4000 - by Bioz Stars, 2026-09

90/100 stars

Images

High Performance Liquid Chromatography:

Article Title: Macrocyclic indole derivatives
Article Snippet: Preparative chiral HPLC method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: Chiralpak AD 5μ 250×30 mm; Eluent A: hexane+0.1 Vol-% trifluoroacetic acid; Eluent B: isopropanol; isocratic: 60-40% runtime 20 min; Flow 50 ml/min; UV 254 nm Analytical chiral HPLC method: Instrument: Agilent HPLC 1260; Säule: Chiralpak AD 3μ 100×4.6 mm; Eluent A: hexane+0.1 Vol-% trifluoroacetic acid; Eluent B: isopropanol; Gradient: 20-50% B in 7 min; Flow 1.4 ml/min; Temperature: 25° C.; DAD 254 nm The preparative chiral HPLC yielded the title compound (46 mg). .. Preparative chiral HPLC method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: Chiralpak AD 5μ 250×30 mm; Eluent A: hexane+0.1 Vol-% trifluoroacetic acid; Eluent B: isopropanol; isocratic: 60-40% runtime 20 min; Flow 50 ml/min; UV 254 nm Analytical chiral HPLC method: Instrument: Agilent HPLC 1260; Säule: Chiralpak AD 3μ 100×4.6 mm; Eluent A: hexane+0.1 Vol-% trifluoroacetic acid; Eluent B: isopropanol; Gradient: 20-50% B in 7 min; Flow 1.4 ml/min; Temperature: 25° C.; DAD 254 nm The preparative chiral HPLC yielded the title compound (46 mg). .. Preparative chiral HPLC method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: XBrigde C18 5μ 150×30 mm; Eluent B: water+0.2 Vol-% aqueous ammonia (32%); Eluent C: acetonitrile; Gradient: 2.5-9.5 min 28-52% C, 9.5-11.5 min 100% C; Flow 50.0 ml/min; UV 254 nm Analytical chiral HPLC method: Instrument: Waters Alliance 2695; column: Chiralpak AD-H 3μ 100×4.6 mm; Eluent A: hexane+0.1 Vol-% trifluoroacetic acid (99%); Eluent B: isopropanol; Gradient: 20-50% B in 7 min; Flow 1.4 ml/min; Temperature: 25° C.; DAD 254 nm

Article Title: Macrocyclic indole derivatives
Article Snippet: .. Preparative Chiral HPLC Method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: Chiralpak IA 5μ 250×30 mm; eluent A: hexan eluent B: 2-propanol; gradient: 20-50% B in 15 min+0.1 Vol-% trifluoroacetic acid; flow 40.0 ml/min; UV 254 nm Analytical Chiral HPLC Method: Instrument: Agilent HPLC 1260; column: Chiralpak IA 3μ 100×4.6 mm; eluent A: hexane+0.1 Vol-% trifluoroacetic acid; eluent B: 2-propanol; gradient: 20-50% B in 7 min; flow 1.4 ml/min; temperature: 25° C.; DAD 254 nm ..

Article Title: Macrocyclic indole derivatives
Article Snippet: .. Preparative chiral HPLC method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: Chiralpak AD 5μ 250×30 mm; eluent A: hexane+0.1 Vol-% trifluoroacetic acid (99%); eluent B: 2-propanol; gradient: 20-50%8 in 20 min; flow 40.0 ml/min; UV 254 nm Analytical chiral HPLC method: Instrument: Agilent HPLC 1260; column: Chiralpak AD 3μ 100×4.6 mm; eluent A: hexane+0.1 Vol-% trifluoroacetic acid (99%); eluent B. ..

Article Title: Macrocyclic chlorine substituted indole derivatives
Article Snippet: This was cooled to ambient temperature and purified by reversed phase chromatography (Biotage isolera, 30 g, SNAP C18 cartridge) using acetonitrile containing 0.1% formic acid and water containing 0.1% formic acid buffer (3:97 to 100:0). .. Preparative Chiral HPLC Method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, Column: Chiralpak ID 5μ 250×30 mm; Eluent A: Water+0.1 Vol-% TFA (99%); Eluent B: Acetonitrile; Isocratic: 50% B; Flow 30.0 mL/min; UV 220 nm Analytical Chiral HPLC Method: Instrument: Agilent HPLC 1260; Column: Chiralpak ID 3μ 100×4.6 mm; Eluent A: Water+0.1 Vol-% TFA (99%); Eluent B: Acetonitrile; Isocratisc: 50% B; Flow 1.4 mL/min; Temperature: 25° C.; DAD 220 nm ..

Article Title: Macrocyclic indole derivatives
Article Snippet: .. Preparative Chiral HPLC Method: Instrument: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000, column: Chiralpak IF 5μ 250×30 mm; eluent A: hexane+0.1 Vol-% trifluoroaceticacid; Eluent B: 2-propanol; gradient: 20-50% B in 20 min; flow 40.0 ml/min; UV 254 nm Analytical Chiral HPLC Method: Instrument: Agilent HPLC 1260; Säule: Chiralpak IF 3μ 100×4.6 mm; eluent A: hexan+0.1 Vol-% trifluoroacetic acid; eluent B: 2-propanol; gradient: 20-50% B In 7 min; flow 1.4 ml/min: temperature: 25° C.; DAD 254 nm ..

Solvent:

Article Title: PTEFb inhibiting macrocyclic compounds
Article Snippet: System: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000 Column: YMC Amylose SA, 5 μm 250 × 30 mm Solvent: tert-Butyl methyl ether/MeOH 1:1 Flow: 40 mL/min Temperature: 25° C. Solution: 20 mg in 1 mL DCM/MeOH 1:1 Injection: 1 × 1 mL Detection: UV 280 nm Retention time in min purity in % yield Example 16 14.1-16.2 99.7% 9.0 mg Diasteroisomer 3 Example 17 16.9-18.9 97.0% 8.3 mg Diasteroisomer 4 .. System: Labomatic HD5000, Labocord-5000; Gilson GX-241, Labcol Vario 4000 Column: YMC Amylose SA, 5 μm 250 × 30 mm Solvent: tert-Butyl methyl ether/MeOH 1:1 Flow: 40 mL/min Temperature: 25° C. Solution: 20 mg in 1 mL DCM/MeOH 1:1 Injection: 1 × 1 mL Detection: UV 280 nm Retention time in min purity in % yield Example 16 14.1-16.2 99.7% 9.0 mg Diasteroisomer 3 Example 17 16.9-18.9 97.0% 8.3 mg Diasteroisomer 4 ..

Review

labcol vario 4000 (Gilson Inc)

Structured Review

Images

Related Articles

High Performance Liquid Chromatography:

Solvent:

Injection:

Similar Products

Image Search Results